4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

Base Information

Chemical Name:4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione
CAS No.:1186335-69-2
Molecular Formula:C₂₃H₁₅Cl₄NO₃
Molecular Weight:495.189
Hs Code.:

Synonyms:4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

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Chemical Property of 4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

Chemical Property:

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Technology Process of 4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

There total 5 articles about 4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1174988-18-1
3-[2-(4-methoxyphenyl)ethyl]aniline

: 117-08-8
tetrachlorophthalic anhydride

: 1186335-69-2
4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

Guidance literature:: at 200 ℃; for 1h; Neat (no solvent);
DOI:10.1016/j.bmc.2009.05.066

Reference yield:

: 3462-97-3
(4-methoxybenzyl)triphenylphosphonium bromide

: 1186335-69-2
4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; 18-crown-6 ether / dichloromethane / Reflux

2: hydrogen; palladium 10% on activated carbon / ethyl acetate / 20 °C

3: acetic acid / Heating

With 18-crown-6 ether; palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; In dichloromethane; ethyl acetate; 1: |Wittig Olefination;
DOI:10.1002/cmdc.201600305

Reference yield:

: 603-35-0
triphenylphosphine

: 1186335-69-2
4,5,6,7-tetrachloro-2-(3-(4-methoxyphenethyl)phenyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 4.5 h / Reflux

2: potassium carbonate; 18-crown-6 ether / dichloromethane / Reflux

3: hydrogen; palladium 10% on activated carbon / ethyl acetate / 20 °C

4: acetic acid / Heating

With 18-crown-6 ether; palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; In dichloromethane; ethyl acetate; acetonitrile; 2: |Wittig Olefination;
DOI:10.1002/cmdc.201600305