<1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

Base Information

Chemical Name:<1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane
CAS No.:119111-16-9
Molecular Formula:C₄₃H₄₄O₆
Molecular Weight:656.819
Hs Code.:

Synonyms:<1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

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Chemical Property of <1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

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Technology Process of <1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

There total 7 articles about <1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-24-7
acetic anhydride

: 119111-15-8
<1R-(1α,2α,3β,4α,5β)>-3-(Methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentanol

: 119111-16-9
<1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

Guidance literature:: With dmap; In pyridine; at 0 ℃;
DOI:10.1021/ja00187a031

Reference yield:

: 119111-14-7
<1S-(1α,2α,3β,4α,5β)>-2-Hydroxy-5-(methoxymethyl)-3,4-bis(phenylmethoxy)cyclopentanemethanol

: 119111-16-9
<1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: pyridine

With pyridine;
DOI:10.1021/ja00236a064

Reference yield:

: 20770-84-7,113566-69-1,113566-70-4
2,3-di-O-benzyl-4,6-O-benzylidene-D-glucopyranose

: 119111-16-9
<1R-(1α,2α,3β,4α,5β)>-1-Acetoxy-3-(methoxymethyl)-4,5-bis(phenylmethoxy)-2-<(triphenylmethoxy)methyl>cyclopentane

Guidance literature:: Multi-step reaction with 6 steps

2: 1,2-dichloro-ethane

3: Bu₃SnH, AIBN / toluene / Heating

4: H₃O⁽¹⁺⁾

5: pyridine

6: pyridine

With pyridine; 2,2'-azobis(isobutyronitrile); oxonium; tri-n-butyl-tin hydride; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja00236a064