(2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine

Base Information

• Chemical Name: (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine
• CAS No.: 1000612-69-0
• Molecular Formula: C₃₂H₃₃NO₄
• Molecular Weight: 495.618

Synonyms:(2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine

Chemical Property of (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine

There total 5 articles about (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2R,3R,4R,5R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-phenyl-3,4-dihydro-2H-pyrrole 1-oxide (1000612-65-6) → (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine (1000612-69-0)

Guidance literature:

With diisobutylaluminium hydride; at 80 ℃;

DOI:10.1016/j.carres.2013.03.017

Reference yield:

(2R,3R,4R,5R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-phenyl-3,4-dihydro-2H-pyrrole 1-oxide (1000612-65-6) → (2R,3R,4R,5R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine (1000612-60-1) + (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine (1000612-69-0)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; at -80 ℃;

DOI:10.1055/s-2007-991059

Reference yield:

(2S,3R,4R)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-2-phenyl-3,4-dihydro-2H-pyrrole 1-oxide (1000612-71-4) → (2S,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine (1000612-72-5) + (2R,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine (1000612-69-0)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; at -80 ℃;

DOI:10.1055/s-2007-991059

upstream raw materials:

(2R,3R,4R,5R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-phenyl-3,4-dihydro-2H-pyrrole 1-oxide

(2S,3R,4R)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-2-phenyl-3,4-dihydro-2H-pyrrole 1-oxide

(2R,3R,4R,5R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine

Downstream raw materials:

(2R,3R,4R,5R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-phenyl-3,4-dihydro-2H-pyrrole 1-oxide

(2S,3R,4R)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-2-phenyl-3,4-dihydro-2H-pyrrole 1-oxide

(2S,3R,4R,5S)-3,4-bis(benzyloxy)-5-(benzyloxymethyl)-1-hydroxy-5-phenylpyrrolidine

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