Technology Process of C53H21BiF10N4
There total 3 articles about C53H21BiF10N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate;
In
tetrahydrofuran; water;
at 25 - 40 ℃;
for 24h;
Inert atmosphere;
DOI:10.1002/ejic.201200697
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; water / Acidic conditions
2: tris(bis(trimethylsilyl)amido)bismuth / tetrahydrofuran
3: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate / tetrahydrofuran; water / 24 h / 25 - 40 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris(bis(trimethylsilyl)amido)bismuth; palladium diacetate;
In
tetrahydrofuran; methanol; water;
3: |Suzuki Coupling;
DOI:10.1002/ejic.201200697
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tris(bis(trimethylsilyl)amido)bismuth / tetrahydrofuran
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate / tetrahydrofuran; water / 24 h / 25 - 40 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris(bis(trimethylsilyl)amido)bismuth; palladium diacetate;
In
tetrahydrofuran; water;
2: |Suzuki Coupling;
DOI:10.1002/ejic.201200697
