methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

Base Information

Chemical Name:methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate
CAS No.:1035563-60-0
Molecular Formula:C₃₀H₄₁N₃O₈
Molecular Weight:571.671
Hs Code.:

Synonyms:methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

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Chemical Property of methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

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Technology Process of methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

There total 3 articles about methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1035563-59-7
methyl 8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1035563-60-0
methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.jconrel.2009.12.001

Reference yield:

: 1035563-58-6
4,6-benzyloxycarbonyl-4-aza-1,6-hexane diamine

: 1035563-60-0
methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 12 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

With triethylamine; In methanol; dichloromethane; 1: Michael condensation;
DOI:10.1016/j.jconrel.2009.12.001

Reference yield:

: 204061-20-1
{2-[(3-Azido-propyl)-benzyloxycarbonyl-amino]-ethyl}-carbamic acid benzyl ester

: 1035563-60-0
methyl 4-tert-butyloxycarbonyl-8,10-benzyloxycarbonyl-4,8-diaza-10-aminodecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: water; trimethylphosphane / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

2: methanol / 12 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

With water; triethylamine; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; 1: Staudinger reaction / 2: Michael condensation;
DOI:10.1016/j.jconrel.2009.12.001