(1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure

Base Information

• Chemical Name: (1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure
• CAS No.: 79936-78-0
• Molecular Formula: C₁₃H₂₂O₄
• Molecular Weight: 245.291

Synonyms:(1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure

Chemical Property of (1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure

Chemical Property:

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Technology Process of (1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure

There total 2 articles about (1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

2-<(1'S,2'S,6'R)-2',6'-dimethyl-2'-(2''-hydroxy-4''-isopropyl)phenyl-6'-triduteriomethyl-cyclohexyl>-essigsauremethylester (79936-77-9) → (1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure (79936-78-0)

Guidance literature:

With potassium permanganate; magnesium sulfate; In acetone; for 2h; Ambient temperature;

DOI:10.1002/hlca.19810640504

Reference yield:

C20H25(2)H3O2 (79936-76-8) → (1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure (79936-78-0)

Guidance literature:

Multi-step reaction with 2 steps

1: conc. HCl / 1.17 h / Heating

2: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

With hydrogenchloride; potassium permanganate; magnesium sulfate; In acetone;

DOI:10.1002/hlca.19810640504

Reference yield: 16.0%

(1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure (79936-78-0) → 2-<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-cyclohexyl>-essigsaure + 2-<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-cyclohexyl>-essigsauremethylester + 2-<(6'R)-2',6'-dimethyl-6'-trideuteriomethyl-1'-hexenyl>-essigsauremethylester + 2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester (79936-79-1)

Guidance literature:

With lead(IV) acetate; In benzene; at 10 - 15 ℃; for 0.2h; Yield given; Irradiation;

DOI:10.1002/hlca.19810640504

upstream raw materials:

2-<(1'S,2'S,6'R)-2',6'-dimethyl-2'-(2''-hydroxy-4''-isopropyl)phenyl-6'-triduteriomethyl-cyclohexyl>-essigsauremethylester

C₂₀H₂₅⁽²⁾H₃O₂

Downstream raw materials:

(1R,1'R)-<16,16,16,16,',16',16'-²H6>-β,β-carotin

(1R,1'R,6ξ)-<16,16,16,16,',16',16'-²H6>-β,ε-carotin

2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-ethan-1-ol

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