chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II)

Base Information

• Chemical Name: chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II)
• CAS No.: 1398531-33-3
• Molecular Formula: C₄₀H₅₆ClNOP₂Ru
• Molecular Weight: 765.361

Synonyms:chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II)

Chemical Property of chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II)

Chemical Property:

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Technology Process of chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II)

There total 3 articles about chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) (157072-60-1,61521-25-3,166941-05-5,16971-33-8) + 4,5-bis[(dicyclohexylphosphanyl)methyl]acridine (1398555-35-5) → chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II) (1398531-33-3)

Guidance literature:

In toluene; at 70 ℃; for 2h; Inert atmosphere;

Reference yield: 74.0%

ruthenium(H)(Cl)(CO)(triphenylphosphine)3 (911495-91-5) + 4,5-bis[(dicyclohexylphosphanyl)methyl]acridine (1398555-35-5) → C40H56ClNOP2Ru (1398531-33-3,1592939-80-4)

Guidance literature:

In toluene; at 70 ℃; for 2h; Schlenk technique; Glovebox; Inert atmosphere;

DOI:10.1021/ja409368a

Reference yield:

→ chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II) (1398531-33-3)

Guidance literature:

In toluene; at 70 ℃; for 2h;

upstream raw materials:

(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II)

4,5-bis[(dicyclohexylphosphanyl)methyl]acridine

ruthenium(H)(Cl)(CO)(triphenylphosphine)3

Downstream raw materials:

C₄₀H₅₇NOP₂Ru

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