N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Base Information

Chemical Name:N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea
CAS No.:130804-53-4
Molecular Formula:C₃₆H₄₄F₂N₄O₃S
Molecular Weight:650.833
Hs Code.:

Synonyms:N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Suppliers and Price of N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

There total 6 articles about N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4,5-[bis-(4-methoxyphenyl)-1H-imidazol]-2-thione

: 130804-30-7
N-(2,4-difluorophenyl)-N'-heptyl-N'-(5-bromopentyl)urea

: 130804-53-4
N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Guidance literature:: In N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 130804-53-4
N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / toluene / 18 h / Heating

2: 85 percent / LiAlH₄ / tetrahydrofuran / 18 h / Heating

3: 97 percent / CH₂Cl₂ / 1 h / 0 °C

4: 100 percent / CBr₄, triphenylphosphine / CH₂Cl₂ / 3 h / Ambient temperature

5: 1.) NaH / 1.) DMF, 0 deg C, 2 h, 2.) DMF, RT, 2 h

With lithium aluminium tetrahydride; carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jm00007a004

Reference yield:

: 111-68-2
1-Heptylamine

: 130804-53-4
N-<5-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>pentyl>-N'-(2,4-difluorophenyl)-N-heptylurea

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / toluene / 18 h / Heating

2: 85 percent / LiAlH₄ / tetrahydrofuran / 18 h / Heating

3: 97 percent / CH₂Cl₂ / 1 h / 0 °C

4: 100 percent / CBr₄, triphenylphosphine / CH₂Cl₂ / 3 h / Ambient temperature

5: 1.) NaH / 1.) DMF, 0 deg C, 2 h, 2.) DMF, RT, 2 h

With lithium aluminium tetrahydride; carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jm00007a004