2--1-(1-phenylethenyl)cyclopentanol

Base Information

Chemical Name:2--1-(1-phenylethenyl)cyclopentanol
CAS No.:87014-64-0
Molecular Formula:C₁₆H₂₀N₂O
Molecular Weight:256.348
Hs Code.:

2-<methyl(cyanomethyl)amino>-1-(1-phenylethenyl)cyclopentanol

Synonyms:2--1-(1-phenylethenyl)cyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--1-(1-phenylethenyl)cyclopentanol

Chemical Property:

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Technology Process of 2--1-(1-phenylethenyl)cyclopentanol

There total 3 articles about 2--1-(1-phenylethenyl)cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87014-74-2
trans-2-(methylamino)cyclopentanol

: 87014-64-0
2--1-(1-phenylethenyl)cyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) HCl / 1.) H₂O, 0 deg C, 2.) room temperature, overnight

2: 1.) Me₂SO, oxalyl chloride, 2.) Et₃N / 1.) methylene dichloride, -60 deg C to -50 deg C, 25 min, 2.) -60 deg C to -50 deg C, 5 min, then to room temperature

3: 1.) t-BuLi / 1.) pentane, ether, -78 deg C, 1 h, 2.) ether, -78 deg C, 2 h

With hydrogenchloride; oxalyl dichloride; tert.-butyl lithium; dimethyl sulfoxide; triethylamine;
DOI:10.1021/ja00360a014

Reference yield:

: 87014-75-3
trans-2-cyclopentanol

: 87014-64-0
2--1-(1-phenylethenyl)cyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Me₂SO, oxalyl chloride, 2.) Et₃N / 1.) methylene dichloride, -60 deg C to -50 deg C, 25 min, 2.) -60 deg C to -50 deg C, 5 min, then to room temperature

2: 1.) t-BuLi / 1.) pentane, ether, -78 deg C, 1 h, 2.) ether, -78 deg C, 2 h

With oxalyl dichloride; tert.-butyl lithium; dimethyl sulfoxide; triethylamine;
DOI:10.1021/ja00360a014

Reference yield:

: 98-81-7
1-bromovinylbenzene

: 87014-62-8
2-cyclopentanone

: 87014-64-0
2--1-(1-phenylethenyl)cyclopentanol

Guidance literature:: With tert.-butyl lithium; Yield given. Multistep reaction; 1.) pentane, ether, -78 deg C, 1 h, 2.) ether, -78 deg C, 2 h;
DOI:10.1021/ja00360a014