<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

Base Information

Chemical Name:<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine
CAS No.:147355-09-7
Molecular Formula:C₃₃H₄₁BrN₈O
Molecular Weight:645.646
Hs Code.:

<3-<N-<2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

Synonyms:<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

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Chemical Property of <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

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Technology Process of <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

There total 11 articles about <3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 147355-08-6
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

: 147355-09-7
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/ja00056a014

Reference yield:

: 68621-88-5
(3-aminophenyl)carbamic acid tert-butyl ester

: 147355-09-7
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

Guidance literature:: Multi-step reaction with 7 steps

1: 68 percent / triethylamine / tetrahydrofuran / 12 h / Heating

2: 90 percent / triethylamine / CH₂Cl₂; toluene / 1 h / Ambient temperature

3: 95 percent / hydrazine / methanol / 4 h / Heating

4: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

5: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

6: 86 percent / diisopropylethylamine / tetrahydrofuran / 4 h / Heating

7: 90 percent / trifluoroacetic acid / CH₂Cl₂ / 2 h / Ambient temperature

With ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; hydrazine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00056a014

Reference yield:

: 147355-04-2
5-bromo-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)benzoic acid

: 147355-09-7
<3--1,3,5-triazin-2-yl>amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>amine

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / 2 h / Heating

2: 90 percent / triethylamine / CH₂Cl₂; toluene / 1 h / Ambient temperature

3: 95 percent / hydrazine / methanol / 4 h / Heating

4: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

5: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

6: 86 percent / diisopropylethylamine / tetrahydrofuran / 4 h / Heating

7: 90 percent / trifluoroacetic acid / CH₂Cl₂ / 2 h / Ambient temperature

With thionyl chloride; ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; hydrazine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00056a014