Technology Process of CH3CN*2Cl(1-)*6CO*2Mo(3+)*4((C6H5)PO)(1-)=(CO)4Mo((C6H5)PO)4Mo(CO)2Cl2CH3CN
There total 1 articles about CH3CN*2Cl(1-)*6CO*2Mo(3+)*4((C6H5)PO)(1-)=(CO)4Mo((C6H5)PO)4Mo(CO)2Cl2CH3CN which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
SOCl2;
In
dichloromethane;
to soln. of Mo-complex at -5°C SOCl2 was added dropwise, stirred for 0.5 h; filtd., cold CH3CN was added to the filtrate, cooled -40°C, ppt. was collected, dried under vac.;;