2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone

Base Information

• Chemical Name: 2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone
• CAS No.: 1310875-58-1
• Molecular Formula: C₂₀H₁₆ClN₃O₂S₂
• Molecular Weight: 429.951

Synonyms:2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone

Chemical Property of 2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone

Chemical Property:

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Technology Process of 2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone

There total 1 articles about 2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

thiazolidine-2-thione (134469-06-0) + 2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)acetic acid (1310875-75-2) → 2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone (1310875-58-1)

Guidance literature:

2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)acetic acid; With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 1h;

thiazolidine-2-thione; With dmap; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/ejoc.201100571

Reference yield: 63.0%

2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)-1-(2-thioxothiazolidin-3-yl)ethanone (1310875-58-1) → 2-[4-chloro-5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy]-1-(2-thioxothiazolidin-3-yl)ethanone (1338378-30-5)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; for 4h; regioselective reaction; Reflux;

DOI:10.1002/ejoc.201100571

upstream raw materials:

thiazolidine-2-thione

2-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy)acetic acid

Downstream raw materials:

2-[4-chloro-5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yloxy]-1-(2-thioxothiazolidin-3-yl)ethanone

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