phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

• Chemical Name: phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
• CAS No.: 122078-53-9
• Molecular Formula: C₂₆H₂₅Cl₂NO₁₁
• Molecular Weight: 598.391

Synonyms:phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property of phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 6 articles about phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.7%

2,6-dichloro-4-aminophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (122078-61-9) + p-benzoquinone (106-51-4) → phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (122078-53-9)

Guidance literature:

With molecular sieve; In 1,4-dioxane; Ambient temperature;

DOI:10.1248/cpb.38.13

Reference yield: 44.1%

2,6-dichloro-4-[(4-hydroxyphenyl)imino]-2,5-cyclohexadien-1-one sodium (620-45-1) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (122078-53-9)

Guidance literature:

With silver(l) oxide; In acetonitrile; at 40 ℃;

DOI:10.1248/cpb.38.13

Reference yield: 10.8%

2,6-Dichlorophenolindophenol (956-48-9) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → 2,6-dichlorophenolindophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (129253-64-1) + phenolindo-3',5'-dichlorophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (122078-53-9)

Guidance literature:

With silver(l) oxide; In benzene; Heating;

DOI:10.1248/cpb.38.13

upstream raw materials:

2,6-dichloro-4-aminophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

p-benzoquinone

2,6-Dichlorophenolindophenol

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Downstream raw materials:

phenolindo-3',5'-dichlorophenyl β-D-glucopyranoside

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