C₂₈H₂₇NO₆

Base Information

Chemical Name:C₂₈H₂₇NO₆
CAS No.:144154-93-8
Molecular Formula:C₂₈H₂₇NO₆
Molecular Weight:473.525
Hs Code.:

C<sub>28</sub>H<sub>27</sub>NO<sub>6</sub>

Synonyms:C₂₈H₂₇NO₆

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Chemical Property of C₂₈H₂₇NO₆

Chemical Property:

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Technology Process of C₂₈H₂₇NO₆

There total 7 articles about C₂₈H₂₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 144127-89-9
C₃₄H₃₇NO₅Si

: 144154-93-8
C₂₈H₂₇NO₆

Guidance literature:: With water; toluene-4-sulfonic acid; In benzene; at 50 ℃; for 2h;
DOI:10.1021/ja00049a022

Reference yield:

: 144154-92-7
C₂₆H₁₉NO₅

: 144154-93-8
C₂₈H₂₇NO₆

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / triethylamine / CH₂Cl₂ / 0.5 h / 20 °C

2: 100 percent / DMAP / CH₂Cl₂ / 48 h / 25 °C

3: 95 percent / n-Bu₃SnH, AIBN / benzene / 1 h / 70 °C

4: 93 percent / cesium carbonate / methanol / 1 h / 40 °C

5: 66 percent / cesium carbonate, 18-crown-6 / acetonitrile / 6 h / 25 °C

6: 71 percent / p-toluenesulfonic acid, water / benzene; various solvent(s) / 2 h / 50 °C

With dmap; 18-crown-6 ether; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; caesium carbonate; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; acetonitrile; benzene;
DOI:10.1021/ja00049a022

Reference yield:

: 144127-88-8
C₂₆H₁₉NO₄

: 144154-93-8
C₂₈H₂₇NO₆

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / cesium carbonate, 18-crown-6 / acetonitrile / 6 h / 25 °C

2: 71 percent / p-toluenesulfonic acid, water / benzene; various solvent(s) / 2 h / 50 °C

With 18-crown-6 ether; water; caesium carbonate; toluene-4-sulfonic acid; In acetonitrile; benzene;
DOI:10.1021/ja00049a022