Technology Process of C47H77NO14
There total 58 articles about C47H77NO14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide;
at 80 ℃;
DOI:10.1016/j.tet.2007.02.044
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide;
at 80 ℃;
Yield given;
DOI:10.1021/ja00014a063
- Guidance literature:
-
Multi-step reaction with 14 steps
1: 95 percent / DMAP
2: NaBH4 / methanol
3: H+
4: H2 / 5percent Pd-C / ethanol
5: LiAlH4
6: 1.) DMAP, 2.) NaH
7: DMAP
8: NaH, Bu4NI
9: Et3N
10: KH, 18-crown-6
11: Bu4NF / tetrahydrofuran / Ambient temperature
12: pyridinium dichromate (PDC) / CH2Cl2
13: NaClO2, 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O
14: Bu4NF / hexamethylphosphoric acid triamide / 80 °C
With
dmap; sodium chlorite; sodium tetrahydroborate; lithium aluminium tetrahydride; dipyridinium dichromate; 2-methyl-but-2-ene; 18-crown-6 ether; tetrabutyl ammonium fluoride; hydrogen; hydrogen cation; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja00014a063
