3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

Base Information

Chemical Name:3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol
CAS No.:930283-70-8
Molecular Formula:C₇₈H₁₁₉NO₉
Molecular Weight:1214.8
Hs Code.:

Synonyms:3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

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Chemical Property of 3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

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Technology Process of 3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

There total 10 articles about 3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930283-68-4
(2R,4aR,6S,7R,8S,8aR)-6-((E)-(2S,3S,4R)-2-Amino-3,4-bis-benzyloxy-octadec-6-enyloxy)-7-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

: C₅₇H₇₅NO₁₀

: 930283-70-8
3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

: C₈₃H₁₂₅NO₁₁

Guidance literature:: 1-hexacosanoic acid; With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In dichloromethane; for 1h;

(2R,4aR,6S,7R,8S,8aR)-6-((E)-(2S,3S,4R)-2-Amino-3,4-bis-benzyloxy-octadec-6-enyloxy)-7-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol; C₅₇H₇₅NO₁₀; In dichloromethane; at 20 ℃;

Reference yield:

: C₈₃H₁₂₅NO₁₁

: 930283-70-8
3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

Guidance literature:: In pyridine; acetic acid; at 20 ℃; for 1.5h;

Reference yield:

: C₆₀H₈₂NO₁₀P

: 506-46-7
1-hexacosanoic acid

: 930283-70-8
3,4-di-O-benzyl-1-O-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-hexacosylamino-D-ribo-octadec-6-en-1-ol

: 4-Oxo-pentanoic acid (2R,4aR,6S,7R,8S,8aS)-7-benzyloxy-6-((E)-(2S,3S,4R)-3,4-bis-benzyloxy-2-hexacosanoylamino-octadec-6-enyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: C₆₀H₈₂NO₁₀P; With sodium hydroxide; for 5h;

1-hexacosanoic acid; With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2005.02.018