N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Base Information

Chemical Name:N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine
CAS No.:816444-64-1
Molecular Formula:C₁₉H₂₂N₂O₅S₂
Molecular Weight:422.526
Hs Code.:

Synonyms:N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Suppliers and Price of N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

There total 4 articles about N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 94892-50-9
(rac)-(-)-N-(p-toluenesulfonyl)-p-toluenesulfonimidamide

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 816444-64-1
N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; iodosylbenzene; In acetonitrile; at -18 ℃; for 24h;
DOI:10.1021/ol048167a

Reference yield:

: 10439-23-3
4-methylbenzenesulfinyl chloride

: 816444-64-1
N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 1.5 h / 80 °C

2: 4.35 g / aq. NH₃ / acetonitrile / 0.75 h / 20 °C

3: 97 percent / Cu(CH₃CN)4PF₆; PhIO / acetonitrile / 24 h / -18 °C

With ammonium hydroxide; tetrakis(actonitrile)copper(I) hexafluorophosphate; iodosylbenzene; In toluene; acetonitrile;
DOI:10.1021/ol048167a

Reference yield:

: 108875-13-4
N-(4-methylbenzenesulfonyl) 4-methylphenyl sulfonimidoyl chloride

: 816444-64-1
N-[N-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-2-methoxycarbonyl-2-methylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 4.35 g / aq. NH₃ / acetonitrile / 0.75 h / 20 °C

2: 97 percent / Cu(CH₃CN)4PF₆; PhIO / acetonitrile / 24 h / -18 °C

With ammonium hydroxide; tetrakis(actonitrile)copper(I) hexafluorophosphate; iodosylbenzene; In acetonitrile;
DOI:10.1021/ol048167a