Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside
CAS No.:116730-84-8
Molecular Formula:C₈₂H₈₇FO₁₅
Molecular Weight:1331.58
Hs Code.:

Synonyms:Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 3 articles about Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.6%

: 53810-61-0
methyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 115175-65-0
(2S,3R,4S,5S,6S)-3,4,5-Tris-benzyloxy-2-fluoro-6-fluoromethyl-tetrahydro-pyran

: 116730-86-0
Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-β-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 116730-84-8
Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver perchlorate; tin(ll) chloride; In diethyl ether; at -20 ℃; for 1h;
DOI:10.1016/0008-6215(88)84143-0

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 116730-84-8
Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: silver perchlorate, 2,4,6-trimethylpyridine / diethyl ether / 0.17 h / -30 °C

2: sodium methoxyde / methanol; toluene / 2 h / Heating

3: 67.6 percent / silver perchlorate, molecular sieves 4A, anhydrous stannous chloride / diethyl ether / 1 h / -20 °C

With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; sodium methylate; silver perchlorate; tin(ll) chloride; In methanol; diethyl ether; toluene;
DOI:10.1016/0008-6215(88)84143-0

Reference yield:

: 38184-15-5
methyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1<*>6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 116730-84-8
Methyl O-(2,3,4-tri-O-benzyl-6-deoxy-6-fluoro-α-D-glucopyranosyl)-(1-6)-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methoxyde / methanol; toluene / 2 h / Heating

2: 67.6 percent / silver perchlorate, molecular sieves 4A, anhydrous stannous chloride / diethyl ether / 1 h / -20 °C

With 4 A molecular sieve; sodium methylate; silver perchlorate; tin(ll) chloride; In methanol; diethyl ether; toluene;
DOI:10.1016/0008-6215(88)84143-0