Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid
CAS No.:112622-68-1
Molecular Formula:C₅₁H₅₇NO₁₃
Molecular Weight:892.012
Hs Code.:

Synonyms:Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

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Chemical Property of Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

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Technology Process of Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

There total 5 articles about Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 112622-66-9
Acetic acid (4aS,6S,7R,8S,8aR)-8-benzyloxy-6-((2R,3S,4R,5R,6S)-4-benzyloxy-5-benzyloxycarbonylamino-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

: 112622-68-1
Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: With hydrogenchloride; molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; at 0 ℃;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 112622-68-1
Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 92 percent / pyridine

3: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

With pyridine; hydrogenchloride; molecular sieve; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 110236-58-3
Methyl-3,6-di-O-benzyl-4-O-(3-O-benzyl-α-L-idopyranosyl)-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

: 112622-68-1
Methyl-4-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 92 percent / pyridine

3: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

With pyridine; hydrogenchloride; molecular sieve; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;