Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

Base Information

Chemical Name:Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester
CAS No.:130849-12-6
Molecular Formula:C₁₉H₂₄NO₂P
Molecular Weight:329.379
Hs Code.:

Synonyms:Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

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Chemical Property of Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

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Technology Process of Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

There total 4 articles about Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-88-3,15644-74-3,16713-13-6
toluene

: 130849-12-6
Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NBS / AIBN / CCl₄

2: 1) LDA / 1) THF, - 75 deg C, 2) r.t., overnight

With N-Bromosuccinimide; lithium diisopropyl amide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane;

Reference yield:

: (Benzylamino-methyl)-methyl-phosphinic acid isopropyl ester

: 130849-12-6
Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C

3: 1) LDA / 1) THF, - 75 deg C, 2) r.t., overnight

With hydrogen; lithium diisopropyl amide; palladium on activated charcoal;

Reference yield:

: Aminomethyl-methyl-phosphinic acid isopropyl ester

: 130849-12-6
Methyl-(2-phenyl-1-{[1-phenyl-meth-(E)-ylidene]-amino}-ethyl)-phosphinic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1) LDA / 1) THF, - 75 deg C, 2) r.t., overnight

With lithium diisopropyl amide;