Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester

Base Information

• Chemical Name: Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester
• CAS No.: 85433-41-6
• Molecular Formula: C₂₈H₂₆F₃NO₆
• Molecular Weight: 529.513

Synonyms:Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester

Chemical Property of Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester

Chemical Property:

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Technology Process of Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester

There total 2 articles about Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzoic acid 5-{2-[2-(3,4-dimethoxy-phenyl)-acetylamino]-ethyl}-2-methoxy-phenyl ester → Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester (85433-41-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) NaBH₄

With sodium tetrahydroborate;

DOI:10.1016/S0040-4039(00)85659-2

Reference yield:

Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-1,2,3,4-tetrahydro-isoquinolin-6-yl ester → Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester (85433-41-6)

Guidance literature:

DOI:10.1016/S0040-4039(00)85659-2

Reference yield: 82.0%

Benzoic acid 1-(3,4-dimethoxy-benzyl)-7-methoxy-2-(2,2,2-trifluoro-acetyl)-1,2,3,4-tetrahydro-isoquinolin-6-yl ester (85433-41-6) → N-trifluoroacetyl neospirinedienone (37657-48-0) + C27H22F3NO6 (85458-10-2)

Guidance literature:

With lithium perchlorate; sodium carbonate; In acetonitrile; at -15 - 0 ℃; 0.9 to 1.0 V, Pt anod; Ag/Ag⁽¹⁺⁾ katod;

DOI:10.1016/S0040-4039(00)85659-2

Downstream raw materials:

N-trifluoroacetyl neospirinedienone

C₂₇H₂₂F₃NO₆

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