C₅₃H₄₈BF₂N₇Si

Base Information

• Chemical Name: C₅₃H₄₈BF₂N₇Si
• CAS No.: 1447766-28-0
• Molecular Formula: C₅₃H₄₈BF₂N₇Si
• Molecular Weight: 859.904
• Mol file: 1447766-28-0.mol

Synonyms:C₅₃H₄₈BF₂N₇Si

Chemical Property of C₅₃H₄₈BF₂N₇Si

Chemical Property:

Purity/Quality:

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Technology Process of C₅₃H₄₈BF₂N₇Si

There total 1 articles about C₅₃H₄₈BF₂N₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

C48H39BF2IN7 (1228675-11-3) + trimethylsilylacetylene (1066-54-2) → C53H48BF2N7Si (1447766-28-0)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In benzene; at 50 ℃; for 18h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201300413

Reference yield: 82.0%

C53H48BF2N7Si (1447766-28-0) → C50H40BF2N7 (1447766-30-4)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201300413

Reference yield:

C53H48BF2N7Si (1447766-28-0) → C70H50BF2I2N7

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / methanol; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Schlenk technique

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / benzene / 18 h / 70 °C / Inert atmosphere; Schlenk technique

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; benzene;

DOI:10.1002/chem.201300413

upstream raw materials:

C₄₈H₃₉BF₂IN₇

trimethylsilylacetylene

Downstream raw materials:

C₅₀H₄₀BF₂N₇