Technology Process of 1-(p-aminophenethyl)ethylenediaminetetra-acetic acid
There total 7 articles about 1-(p-aminophenethyl)ethylenediaminetetra-acetic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
ethanol;
under 760 Torr;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) borane, 2.) triethylamine / 1.) THF, 60 deg C, 2.) acetonitrile, room temperature, 50 deg C, 24 h
2: 41 percent / 95percent HNO3 / 3 h / -40 °C
3: conc. HCl / acetic acid / 20 h / Heating
4: 71 percent / KOH / H2O / 50 °C / pH 9.5-10.5
5: hydrogen, triethylamine / 10percent Pd-charcoal / ethanol / 760 Torr / Ambient temperature
With
hydrogenchloride; potassium hydroxide; borane; hydrogen; nitric acid; triethylamine;
palladium on activated charcoal;
In
ethanol; water; acetic acid;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 88 percent / thionyl chloride / 72 h / Ambient temperature
2: 1.) aq. Na2CO3, 2.) ammonia / 1.) water, 2.) methanol, room temperature, 48 h
3: 1.) borane, 2.) triethylamine / 1.) THF, 60 deg C, 2.) acetonitrile, room temperature, 50 deg C, 24 h
4: 41 percent / 95percent HNO3 / 3 h / -40 °C
5: conc. HCl / acetic acid / 20 h / Heating
6: 71 percent / KOH / H2O / 50 °C / pH 9.5-10.5
7: hydrogen, triethylamine / 10percent Pd-charcoal / ethanol / 760 Torr / Ambient temperature
With
hydrogenchloride; potassium hydroxide; thionyl chloride; borane; ammonia; hydrogen; nitric acid; sodium carbonate; triethylamine;
palladium on activated charcoal;
In
ethanol; water; acetic acid;
