C₂₆H₃₃FN₂O₅Si

Base Information

Chemical Name:C₂₆H₃₃FN₂O₅Si
CAS No.:1371641-75-6
Molecular Formula:C₂₆H₃₃FN₂O₅Si
Molecular Weight:500.642
Hs Code.:

C<sub>26</sub>H<sub>33</sub>FN<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₂₆H₃₃FN₂O₅Si

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Chemical Property of C₂₆H₃₃FN₂O₅Si

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Technology Process of C₂₆H₃₃FN₂O₅Si

There total 6 articles about C₂₆H₃₃FN₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1371641-74-5
C₂₆H₃₄N₂O₆Si

: 1371641-75-6
C₂₆H₃₃FN₂O₅Si

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 0 - 23 ℃; for 1.5h;

Reference yield:

: 1253799-71-1
((4aS,8aS,9S)-3-(benzyloxy)-5-((tert-butyldimethylsilyl)oxy)-9-(dimethylamino)-4a-hydroxy-8a,9-dihydronaphtho[2,3-d]isoxazol-4(4aH)-one)

: 1371641-75-6
C₂₆H₃₃FN₂O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1: N-iodo-succinimide / acetonitrile; water / 4.5 h / -10 - 0 °C / Darkness

2: silver trifluoroacetate / 1,4-dioxane; water / 13 h / 23 - 40 °C

3: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 4 h / 0 - 23 °C

4: hydrogenchloride; water / methanol / 4 h / 23 °C

5: diethylamino-sulfur trifluoride / dichloromethane / 1.5 h / 0 - 23 °C

With hydrogenchloride; N-iodo-succinimide; diethylamino-sulfur trifluoride; water; silver trifluoroacetate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 1371641-69-8
C₂₆H₃₃IN₂O₅Si

: 1371641-75-6
C₂₆H₃₃FN₂O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: silver trifluoroacetate / 1,4-dioxane; water / 13 h / 23 - 40 °C

2: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 4 h / 0 - 23 °C

3: hydrogenchloride; water / methanol / 4 h / 23 °C

4: diethylamino-sulfur trifluoride / dichloromethane / 1.5 h / 0 - 23 °C

With hydrogenchloride; diethylamino-sulfur trifluoride; water; silver trifluoroacetate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene;