Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

Base Information

Chemical Name:Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid
CAS No.:80840-58-0
Molecular Formula:C₂₆H₃₀N₄O₃S*HI
Molecular Weight:606.528
Hs Code.:

Synonyms:Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

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Chemical Property of Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

Chemical Property:

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Technology Process of Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

There total 8 articles about Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 80853-56-1
4-[3-(4-Methyl-piperidin-1-yl)-2-(naphthalene-2-sulfonylamino)-3-oxo-propyl]-thiobenzimidic acid methyl ester; hydriodide

: 80840-58-0
Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

Guidance literature:: With ammonium acetate; In ethanol; at 70 - 80 ℃; for 2.5h;

Reference yield:

: 52117-01-8
N-acetyl-4-cyano-α-(ethoxycarbonyl)phenylalanine ethyl ester

: 80840-58-0
Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

Guidance literature:: Multi-step reaction with 6 steps

2: SOCl₂ / 1 h / Heating

3: 89 percent / benzene / 1.5 h / Ambient temperature

4: 99 percent / H₂S (gas), TEA / pyridine / 72 h / Ambient temperature

5: 82.5 percent / acetone / 27 h / Ambient temperature

6: 89 percent / Ammonium acetate / ethanol / 2.5 h / 70 - 80 °C

With ammonium acetate; thionyl chloride; TEA; hydrogen sulfide; In pyridine; ethanol; acetone; benzene;

Reference yield:

: 93-11-8
2-Naphthalenesulfonyl chloride

: 80840-58-0
Nα-(2-Naphthylsulfonyl)-4-amidinophenylalanin-4'-methylpiperididhydroiodid

Guidance literature:: Multi-step reaction with 6 steps

2: SOCl₂ / 1 h / Heating

3: 89 percent / benzene / 1.5 h / Ambient temperature

4: 99 percent / H₂S (gas), TEA / pyridine / 72 h / Ambient temperature

5: 82.5 percent / acetone / 27 h / Ambient temperature

6: 89 percent / Ammonium acetate / ethanol / 2.5 h / 70 - 80 °C

With ammonium acetate; thionyl chloride; TEA; hydrogen sulfide; In pyridine; ethanol; acetone; benzene;