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Technology Process of (C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4

(C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4

Base Information
  • Chemical Name:(C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4
  • CAS No.:207301-27-7
  • Molecular Formula:BF4*C19H19FeN4
  • Molecular Weight:446.038
  • Hs Code.:
(C<sub>6</sub>H<sub>5</sub>)CN<sub>4</sub>H(CH(CH<sub>3</sub>)(C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>5</sub>))<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=[C<sub>6</sub>H<sub>5</sub>CN<sub>4</sub>H(CH(CH<sub>3</sub>)(C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>5</sub>))]BF<sub>4</sub>

Synonyms:(C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4

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Chemical Property of (C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4
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Technology Process of (C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4

There total 1 articles about (C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

tetrafluoroboric acid

tetrafluoroboric acid

5-Phenyl-1H-tetrazole
18039-42-4,3999-10-8

5-Phenyl-1H-tetrazole

1-ferrocenylethanol
1277-49-2

1-ferrocenylethanol

(C<sub>6</sub>H<sub>5</sub>)CN<sub>4</sub>H(CH(CH<sub>3</sub>)(C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>5</sub>))<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=[C<sub>6</sub>H<sub>5</sub>CN<sub>4</sub>H(CH(CH<sub>3</sub>)(C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>5</sub>))]BF<sub>4</sub>
207301-27-7

(C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4

Guidance literature:
In dichloromethane; water; aq. soln. of HBF4 addn. to soln. of Fe-compd. and tetrazole in CH2Cl2 with vigorous stirring, reaction time 15 min; hexane-diethyl ether addn., ppt. filtration off, washing (cooled water),vacuum drying (over P2O5); elem. anal.;

Reference yield:

(C<sub>6</sub>H<sub>5</sub>)CN<sub>4</sub>H(CH(CH<sub>3</sub>)(C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>5</sub>))<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=[C<sub>6</sub>H<sub>5</sub>CN<sub>4</sub>H(CH(CH<sub>3</sub>)(C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>5</sub>))]BF<sub>4</sub>
207301-27-7

(C6H5)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[C6H5CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4

5-Phenyl-1H-tetrazole
18039-42-4,3999-10-8

5-Phenyl-1H-tetrazole

1-ferrocenylethanol
1277-49-2

1-ferrocenylethanol

Guidance literature:
With sodium hydroxide; In water; refluxing (5-10 min), cooling to 5 to 7°C; ppt. filtration off, washing (hot pentane), Fe-compd. obtaining from pentane extracts by drying, tetrazole remaining in the solid residue;
upstream raw materials:

5-Phenyl-1H-tetrazole

1-ferrocenylethanol

Downstream raw materials:

5-Phenyl-1H-tetrazole

1-ferrocenylethanol

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