Technology Process of C32H41N5O4S
There total 4 articles about C32H41N5O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C37H49N5O6S;
With
hydrogenchloride;
In
1,4-dioxane; methanol;
for 2h;
With
sodium carbonate;
In
water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoromethylsulfonic anhydride; triethylamine / dichloromethane / 1 h / -50 °C / Inert atmosphere
1.2: 16 h / 20 °C
2.1: sodium hydroxide; water / 1,4-dioxane / 2 h / pH 13
2.2: pH 7
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h
3.2: 16 h
4.1: hydrogenchloride / 1,4-dioxane; methanol / 2 h
With
hydrogenchloride; trifluoromethylsulfonic anhydride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide; water / 1,4-dioxane / 2 h / pH 13
1.2: pH 7
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h
2.2: 16 h
3.1: hydrogenchloride / 1,4-dioxane; methanol / 2 h
With
hydrogenchloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
1,4-dioxane; methanol; N,N-dimethyl-formamide;
