Technology Process of C46H30F8N2O7S
There total 8 articles about C46H30F8N2O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone
2: water; sodium hydroxide
3: 1,2-dichloro-ethane; dmap / dichloromethane
4: trifluoroacetic acid / dichloromethane
With
dmap; water; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1,2-dichloro-ethane; trifluoroacetic acid; sodium hydroxide;
In
dichloromethane; acetone;
DOI:10.1016/j.molcata.2014.02.030
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydride / N,N-dimethyl-formamide
2: lithium aluminium tetrahydride / tetrahydrofuran
3: triphenylphosphine; tetrachloromethane / acetonitrile
4: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone
5: water; sodium hydroxide
6: 1,2-dichloro-ethane; dmap / dichloromethane
7: trifluoroacetic acid / dichloromethane
With
tetrachloromethane; dmap; lithium aluminium tetrahydride; water; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; 1,2-dichloro-ethane; triphenylphosphine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/j.molcata.2014.02.030
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triphenylphosphine; tetrachloromethane / acetonitrile
2: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone
3: water; sodium hydroxide
4: 1,2-dichloro-ethane; dmap / dichloromethane
5: trifluoroacetic acid / dichloromethane
With
tetrachloromethane; dmap; water; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1,2-dichloro-ethane; triphenylphosphine; trifluoroacetic acid; sodium hydroxide;
In
dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.molcata.2014.02.030