Technology Process of C32H33N3O8
There total 6 articles about C32H33N3O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 1h;
DOI:10.1002/ejoc.201001629
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C
2: triethylamine / dichloromethane / 1 h / 23 °C
3: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine / N,N-dimethyl-formamide / 1 h / 50 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; trifluorormethanesulfonic acid; palladium diacetate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
3: Gassman synthesis;
DOI:10.1002/ejoc.201001629
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h / 20 °C
2: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C
3: triethylamine / dichloromethane / 1 h / 23 °C
4: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine / N,N-dimethyl-formamide / 1 h / 50 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; trifluorormethanesulfonic acid; palladium diacetate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
4: Gassman synthesis;
DOI:10.1002/ejoc.201001629
