3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol

Base Information

• Chemical Name: 3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol
• CAS No.: 1227612-98-7
• Molecular Formula: C₁₀₄H₁₄₀N₂O₂₀
• Molecular Weight: 1738.26

Synonyms:3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol

Chemical Property of 3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol

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Technology Process of 3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol

There total 2 articles about 3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-D-glucopyranosyl)-(1->3)-(4-benzyloxycarbonylamino-2,4,6-trideoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol + acetic anhydride (108-24-7) → 3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol (1227612-98-7)

Guidance literature:

With triethylamine; zinc; at 20 ℃; for 14h;

DOI:10.1002/chem.201001204

Reference yield: 86.0%

3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(4-benzyloxycarbonylamino-2,4,6-trideoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol (1259298-57-1) + acetic anhydride (108-24-7) → 3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol (1227612-98-7)

Guidance literature:

With zinc; Sonication;

DOI:10.1002/anie.200906163

Reference yield: 79.0%

3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol (1227612-98-7) → 3-O-[(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol (1227613-00-4)

Guidance literature:

With methanol; palladium dichloride; In dichloromethane;

DOI:10.1002/anie.200906163

upstream raw materials:

3-O-[(6-O-allyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(4-benzyloxycarbonylamino-2,4,6-trideoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol

acetic anhydride

Downstream raw materials:

3-O-[(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-(2-acetylamino-4-benzyloxycarbonylamino-2,4,6-trideoxy-β-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)]-1,2-di-O-myristoyl-sn-glycerol

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