3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester

Base Information

• Chemical Name: 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester
• CAS No.: 1025926-55-9
• Molecular Formula: C₃₀H₄₃NO₄
• Molecular Weight: 481.676

Synonyms:3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester

Chemical Property of 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester

Chemical Property:

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Technology Process of 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester

There total 1 articles about 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[4-(3-Isopropoxy-phenyl)-butyl]-phenol + 1-t-butoxycarbonyl-3-(p-toluenesulfonyloxymethyl)piperidine (191092-05-4) → 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester (1025926-55-9)

Guidance literature:

With potassium tert-butylate; Multistep reaction; 1.) DMA, 0 deg C, 10 min, 2.) DMA, RT, overnight;

DOI:10.1248/cpb.46.639

Reference yield: 84.0%

3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester (1025926-55-9) → 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine; hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 5h; Ambient temperature;

DOI:10.1248/cpb.46.639

Reference yield:

3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-piperidine-1-carboxylic acid tert-butyl ester (1025926-55-9) → 3-{2-[4-(3-Isopropoxy-phenyl)-butyl]-phenoxymethyl}-1-methyl-piperidine

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.5h; Heating;

DOI:10.1248/cpb.46.639

upstream raw materials:

1-t-butoxycarbonyl-3-(p-toluenesulfonyloxymethyl)piperidine

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