2-Ethyl-N-hydroxybenzimidoyl chloride

Base Information

• Chemical Name: 2-Ethyl-N-hydroxybenzimidoyl chloride
• CAS No.: 1219938-34-7
• Molecular Formula: C₉H₁₀ClNO
• Molecular Weight: 183.637
• Mol file: 1219938-34-7.mol

Synonyms:2-Ethyl-N-hydroxybenzimidoyl chloride

Chemical Property of 2-Ethyl-N-hydroxybenzimidoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-Ethyl-N-hydroxybenzimidoyl chloride

There total 1 articles about 2-Ethyl-N-hydroxybenzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

→ 2-Ethyl-N-hydroxybenzimidoyl chloride (1219938-34-7)

Guidance literature:

With N-chloro-succinimide; N,N-dimethyl-formamide; In 1,2-dichloro-ethane; at 20 - 24 ℃; for 3h;

Reference yield: 96.0%

2-Ethyl-N-hydroxybenzimidoyl chloride (1219938-34-7) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) → 3-(2-ethylphenyl)-1,2-benzisoxazole (1219938-35-8)

Guidance literature:

2-Ethyl-N-hydroxybenzimidoyl chloride; anthranilic acid; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.0833333h;

With tert.-butylnitrite; In acetonitrile; at 20 - 120 ℃; for 0.175h; Microwave irradiation;

DOI:10.1039/b927235f

Reference yield: 96.0%

2-Ethyl-N-hydroxybenzimidoyl chloride (1219938-34-7) + fluorure de dibromo-1,2 ethanesulfonyle (103020-97-9) → 3-(2-ethylphenyl)isoxazole-5-sulfonyl fluoride

Guidance literature:

fluorure de dibromo-1,2 ethanesulfonyle; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

2-Ethyl-N-hydroxybenzimidoyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

DOI:10.1039/c8cc03400a

Downstream raw materials:

3-(2-ethylphenyl)-1,2-benzisoxazole