2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

Base Information

Chemical Name:2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin
CAS No.:150982-72-2
Molecular Formula:C₂₈H₂₄N₂O₃
Molecular Weight:436.51
Hs Code.:

Synonyms:2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

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Chemical Property of 2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

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Technology Process of 2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

There total 3 articles about 2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 844-25-7,55839-33-3
2-benzoyl-1-cyano-1,2-dihydroisoquinoline

: 150982-69-7
2-(2-bromomethyl-phenyl)-2-methyl-[1,3]dioxolane

: 150982-72-2
2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

Guidance literature:: With sodium hydroxide; cetyltrimethylammonim bromide; In benzene; for 26h; Ambient temperature;
DOI:10.1002/ardp.19933260502

Reference yield:

: 150982-68-6
2-methyl-2-(2-methylphenyl)-1,3-dioxolane

: 150982-72-2
2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / NBS, wet benzoyl peroxide / 0.42 h / Heating

2: 73 percent / 50 percent aq. NaOH, cetrimonium bromide / benzene / 26 h / Ambient temperature

With sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; cetyltrimethylammonim bromide; In benzene;
DOI:10.1002/ardp.19933260502

Reference yield:

: 577-16-2,122382-54-1
2-Methylacetophenone

: 150982-72-2
2-Benzoyl-1-<2-(2-methyl-1,3-dioxolan-2-yl)benzyl>-1-cyan-1,2-dihydroisochinolin

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / pyridinium toluene-4-sulfonate / benzene / 14 h / Heating

2: 53 percent / NBS, wet benzoyl peroxide / 0.42 h / Heating

3: 73 percent / 50 percent aq. NaOH, cetrimonium bromide / benzene / 26 h / Ambient temperature

With sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; cetyltrimethylammonim bromide; pyridinium p-toluenesulfonate; In benzene;
DOI:10.1002/ardp.19933260502