Technology Process of C33H41FO9
There total 9 articles about C33H41FO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 80 percent / TsOH / methanol
2: 49 percent / Ac2O
3: 64 percent / NIS; DAST / CH2Cl2 / 1 h / 0 °C
4: 80 percent / HF*Py
5: 97 percent / hydrazine / ethanol
6: 91 percent / n-BuLi
7: 50 percent / (TMS)3SiH; AIBN / toluene
8: 77 percent / NaBH4 / tetrahydrofuran
9: 79 percent / n-Bu3P
10: 71 percent / mCPBA
With
sodium tetrahydroborate; N-iodo-succinimide; n-butyllithium; 2,2'-azobis(isobutyronitrile); tributylphosphine; tris-(trimethylsilyl)silane; acetic anhydride; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 3-chloro-benzenecarboperoxoic acid; 4,4'-diaminostilbene-2,2'-disulfonic acid; hydrazine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; toluene;
DOI:10.1016/S0960-894X(00)00682-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / n-BuLi
2: 50 percent / (TMS)3SiH; AIBN / toluene
3: 77 percent / NaBH4 / tetrahydrofuran
4: 79 percent / n-Bu3P
5: 71 percent / mCPBA
With
sodium tetrahydroborate; n-butyllithium; 2,2'-azobis(isobutyronitrile); tributylphosphine; tris-(trimethylsilyl)silane; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; toluene;
DOI:10.1016/S0960-894X(00)00682-X