benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

Base Information

Chemical Name:benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate
CAS No.:956235-04-4
Molecular Formula:C₂₀H₁₉N₃O₄
Molecular Weight:365.389
Hs Code.:

Synonyms:benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

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Chemical Property of benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

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Technology Process of benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

There total 1 articles about benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 7424-91-1
methyl 3,3-dimethoxypropionate

: 956235-04-4
benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

Guidance literature:: methyl-(3-ureido-benzyl)-carbamic acid benzyl ester; With sodium hydride; In 1,4-dioxane; at 60 ℃; for 1.5h;

methyl 3,3-dimethoxypropionate; In 1,4-dioxane; at 20 ℃; for 1.5h; Heating / reflux;

With sodium hydrogencarbonate; acetic acid; more than 3 stages;

Reference yield: 71.0%

: 956235-04-4
benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

: 956235-05-5
1-{3-[(methylamino)methyl]phenyl}pyrimidine-2,4(1H,3H)-dione

Guidance literature:: benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate; With hydrogenchloride; In ethanol; for 0.5h; Heating / reflux;

With ammonia; In methanol; chloroform; water;

Reference yield:

: 956235-04-4
benzyl [3-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)benzyl]methylcarbamate

: 1-(3-{[{2-[(6-{[(2R)-2-hydroxy-2-(8-hydroxy-2-oxo-1,2-dihydroquinolin-5-yl)ethyl]amino}hexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / ethanol / 0.5 h / Heating / reflux

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 21 h / 70 °C

3: hydrazine / ethanol / 18 h / 20 °C

4: sodium hydrogencarbonate / sodium iodide / dimethyl sulfoxide / 1 h / 140 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 40 °C

6: hydrogen / palladium 10% on activated carbon / methanol / 156 h / 20 °C

With hydrogenchloride; tetrabutyl ammonium fluoride; hydrogen; sodium hydrogencarbonate; hydrazine; palladium 10% on activated carbon; sodium iodide; In tetrahydrofuran; methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;