cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol

Base Information

• Chemical Name: cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol
• CAS No.: 1350724-53-6
• Molecular Formula: C₃₅H₅₄O₅
• Molecular Weight: 554.811
• Mol file: 1350724-53-6.mol

Synonyms:cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol

Chemical Property of cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol

There total 4 articles about cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

C20H31BrO3 + 5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene (56469-10-4) → cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol (1350724-53-6)

Guidance literature:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene; With potassium fluoride; potassium carbonate; In acetone; for 0.5h; Reflux; Inert atmosphere;

C₂₀H₃₁BrO₃; In acetone; for 48h; Reflux; Inert atmosphere;

DOI:10.1021/jm200529h

Reference yield:

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene (60526-81-0) → cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol (1350724-53-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

With potassium fluoride; boron tribromide; potassium carbonate; In dichloromethane; acetone;

DOI:10.1021/jm200529h

Reference yield:

cis-5-hydroxyl-2-phenyl-1,3-dioxane (1708-40-3,4141-19-9,4141-20-2) → cis-3-(2-methyloctan-2-yl)-5-[10-(2-phenyl-1,3-dioxan-5-yloxy)decyloxy]phenol (1350724-53-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: Reflux; Inert atmosphere

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

With potassium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1021/jm200529h

upstream raw materials:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

1,10-dibromodecane

cis-5-hydroxyl-2-phenyl-1,3-dioxane

Downstream raw materials:

2-{10-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]decyloxy}propane-1,3-diol