Technology Process of C27H36N2OSn
There total 5 articles about C27H36N2OSn which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
bis-triphenylphosphine-palladium(II) chloride;
In
1,4-dioxane;
at 80 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / tetrahydrofuran / -78 °C
1.2: 4 h / 20 °C
2.1: boron tribromide / hexane; dichloromethane / 0 °C
2.2: 0 °C
3.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 4 h / 80 °C / Inert atmosphere
With
tert.-butyl lithium; boron tribromide;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: phosphate potassium salt; N,N`-dimethylethylenediamine / copper(l) iodide / toluene / 110 °C / Inert atmosphere
2.1: tert.-butyl lithium / tetrahydrofuran / -78 °C
2.2: 4 h / 20 °C
3.1: boron tribromide / hexane; dichloromethane / 0 °C
3.2: 0 °C
4.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 4 h / 80 °C / Inert atmosphere
With
phosphate potassium salt; tert.-butyl lithium; boron tribromide; N,N`-dimethylethylenediamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; toluene;