4-methoxyphenacylamine ethylene ketal

Base Information

Chemical Name:4-methoxyphenacylamine ethylene ketal
CAS No.:344334-51-6
Molecular Formula:C₁₁H₁₅NO₃
Molecular Weight:209.245
Hs Code.:

Synonyms:4-methoxyphenacylamine ethylene ketal

Suppliers and Price of 4-methoxyphenacylamine ethylene ketal

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Chemical Property of 4-methoxyphenacylamine ethylene ketal

Chemical Property:

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Technology Process of 4-methoxyphenacylamine ethylene ketal

There total 5 articles about 4-methoxyphenacylamine ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 947594-57-2
4-methoxyphenacyl azide ethylene ketal

: 344334-51-6
4-methoxyphenacylamine ethylene ketal

Guidance literature:: 4-methoxyphenacyl azide ethylene ketal; With triphenylphosphine; In tetrahydrofuran;

With water; In tetrahydrofuran; Further stages.;
DOI:10.1021/jm0703035

Reference yield:

: 74730-53-3
2-[2-(4-methoxyphenyl)-1,3-dioxolan-2-ylmethyl]-1H-isoindole-1,3(2H)-dione

: 344334-51-6
4-methoxyphenacylamine ethylene ketal

Guidance literature:: 2-[2-(4-methoxyphenyl)-1,3-dioxolan-2-ylmethyl]-1H-isoindole-1,3(2H)-dione; With hydrazine; for 48h; Heating / reflux;

With sodium hydroxide; In diethyl ether; water; at 20 ℃; for 16h;

Reference yield:

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 344334-51-6
4-methoxyphenacylamine ethylene ketal

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / sodium azide / dimethylsulfoxide / 20 °C

2.1: 70 percent / boron trifluoride etherate / CH₂Cl₂ / 20 °C

3.1: triphenylphosphine / tetrahydrofuran

3.2: 61 percent / water / tetrahydrofuran

With sodium azide; boron trifluoride diethyl etherate; triphenylphosphine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 3.1: Staudinger reaction;
DOI:10.1021/jm0703035