phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

Base Information

Chemical Name:phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose
CAS No.:613247-78-2
Molecular Formula:C₃₉H₇₄O₅SeSi₃
Molecular Weight:786.23
Hs Code.:

Synonyms:phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

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Chemical Property of phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

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Technology Process of phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

There total 3 articles about phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 613247-76-0
phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranoside

: 613247-78-2
phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jo030128+

Reference yield:

: 4981-97-9
phenyl 1-seleno-β-D-glucopyranoside

: 613247-78-2
phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NaH / tetrahydrofuran / 2 h / 20 °C

2: 70 percent / trifluoroacetic acid / tetrahydrofuran; H₂O / 6 h / 20 °C

3: 93 percent / Dess-Martin reagent / CH₂Cl₂ / 0.5 h / 20 °C

With sodium hydride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; 3: Dess-Martin oxidation;
DOI:10.1021/jo030128+

Reference yield:

: 374115-44-3
phenyl 1-seleno-2,3,4,6-tetrakis(O-triisopropylsilyl)-β-D-glucopyranoside

: 613247-78-2
phenyl 1-seleno-2,3,4-tris(O-triisopropylsilyl)-β-D-glucopyranosid-6-urose

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / trifluoroacetic acid / tetrahydrofuran; H₂O / 6 h / 20 °C

2: 93 percent / Dess-Martin reagent / CH₂Cl₂ / 0.5 h / 20 °C

With Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; 2: Dess-Martin oxidation;
DOI:10.1021/jo030128+