N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

Base Information

Chemical Name:N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester
CAS No.:129243-65-8
Molecular Formula:C₂₂H₂₈N₂O₆
Molecular Weight:416.474
Hs Code.:

Synonyms:N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

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Chemical Property of N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

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Technology Process of N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

There total 7 articles about N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3072-56-8
2-(diethylaminomethyl)pyrrole

: 129243-65-8
N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / ethanol / 2 h

2: 1) Na, EtOH / 2) reflux, 2h

3: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

4: 74 percent / 1M NaOH / ethanol / 2 h

5: 99 percent / dioxane / 16 h / Heating

With dmap; sodium hydroxide; ethanol; sodium; In 1,4-dioxane; ethanol; acetonitrile;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 129243-65-8
N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

2: 74 percent / 1M NaOH / ethanol / 2 h

3: 99 percent / dioxane / 16 h / Heating

With dmap; sodium hydroxide; In 1,4-dioxane; ethanol; acetonitrile;

Reference yield:

: 3005-66-1
diethyl 2-benzyloxycarbonylaminomalonate

: 129243-65-8
N(α)-benzyloxycarbonyl-β-2-(N-t-butoxycarbonyl)-pyrrolalanine ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Na, EtOH / 2) reflux, 2h

2: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

3: 74 percent / 1M NaOH / ethanol / 2 h

4: 99 percent / dioxane / 16 h / Heating

With dmap; sodium hydroxide; ethanol; sodium; In 1,4-dioxane; ethanol; acetonitrile;