Technology Process of C23H32O2Si
There total 4 articles about C23H32O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
dichloromethane;
at 0 - 20 ℃;
for 14h;
Inert atmosphere;
DOI:10.1021/ol302409g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triphenylphosphine; tetrachloromethane / 24 h / 80 °C / Inert atmosphere
2: (DHQD)2PHAL; methanesulfonamide; potassium osmate(VI) dihydrate; potassium hexacyanoferrate(III); potassium carbonate; sodium hydrogencarbonate / tert-butyl alcohol; water / 4 h / 0 °C / Inert atmosphere
3: sodium hydroxide / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
4: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
With
(DHQD)2PHAL; 1H-imidazole; tetrachloromethane; potassium osmate(VI) dihydrate; methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; potassium hexacyanoferrate(III);
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
2: |Sharpless Dihydroxylation;
DOI:10.1021/ol302409g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
2: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
With
1H-imidazole; sodium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol302409g
