benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside

Base Information

Chemical Name:benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside
CAS No.:1352410-48-0
Molecular Formula:C₉₂H₁₀₄O₂₂
Molecular Weight:1561.82
Hs Code.:

Synonyms:benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside

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Chemical Property of benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside

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Technology Process of benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside

There total 1 articles about benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1185741-89-2
2-methyl-5-tert-butylphenyl 2,4-di-O-acetyl-1-thio-α-L-rhamnopyranoside

: 1268673-21-7
benzyl 3-O-3,4-di-O-benzoyl-β-D-xylopyranosyloleanolate

: 432519-23-8
2,3,4-tri-O-benzoyl-α-D-xylopyranosyl trichloroacetimidate

: 1352410-48-0
benzyl oleanolate 3β-O-2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1 → 3)-2,4-di-O-acetyl-α-L-rhamnopyranosyl-(1 → 2)-3,4-di-O-benzoyl-β-D-xylopyranoside

Guidance literature:: 2-methyl-5-tert-butylphenyl 2,4-di-O-acetyl-1-thio-α-L-rhamnopyranoside; 2,3,4-tri-O-benzoyl-α-D-xylopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

benzyl 3-O-3,4-di-O-benzoyl-β-D-xylopyranosyloleanolate; With N-iodo-succinimide; In dichloromethane; at -10 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.ejmech.2013.04.016