benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-...

Base Information

• Chemical Name: benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-...
• CAS No.: 153805-01-7
• Molecular Formula: C₁₁₆H₁₁₂N₆O₂₄
• Molecular Weight: 1974.19

Synonyms:benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-...

Chemical Property of benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-...

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-...

There total 2 articles about benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

benzyl 3-O-benzyl-2-deoxy-4-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-phthalimido-6-O-pivaloyl-β-D-glucopyranoside (153805-00-6) + 4-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl trichloroacetoimidate (153804-95-6) → benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-... (153805-01-7)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -15 ℃; for 3h;

DOI:10.1016/S0040-4039(00)61560-5

Reference yield: 50.0%

4-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-D-glucopyranosyl chloride (153804-94-5) + benzyl 3-O-benzyl-2-deoxy-4-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-phthalimido-6-O-pivaloyl-β-D-glucopyranoside (153805-00-6) → benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-... (153805-01-7)

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 6h;

DOI:10.1016/S0040-4039(00)61560-5

Reference yield:

acetic anhydride (108-24-7) + benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-... (153805-01-7) → benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(2''-acetimido-3'',6''-di-O-benzyl-2''-deoxy-D-glucopyranosyl)-(1-4)-O-(2'-acetimido-3',6'-di-O-benzyl-2'-deoxy-β-D-glucopyranosyl)(1-4)-2-acetimido-3-O-benzyl-...

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)61560-5

upstream raw materials:

4-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-D-glucopyranosyl chloride

benzyl 3-O-benzyl-2-deoxy-4-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-phthalimido-6-O-pivaloyl-β-D-glucopyranoside

4-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl trichloroacetoimidate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 153805-01-7 benzyl O-(2'''-azido-3''',4''',6'''-tri-O-benzyl-2'''-deoxy-β-D-glucopyranosyl)-(1-4)-O-(3'',6''-di-O-benzyl-2''-deoxy-2''-phthalimido-D-glucopyranosyl)-(1-4)-O-(3',6'-di-O-benzyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)(1-4)-3-O-benzyl-2-deoxy-...

Send

Send

Metric Ton KG G Pound L ML

Send

Send