C₆₉H₆₂O₁₄

Base Information

Chemical Name:C₆₉H₆₂O₁₄
CAS No.:1599469-73-4
Molecular Formula:C₆₉H₆₂O₁₄
Molecular Weight:1115.24
Hs Code.:

C<sub>69</sub>H<sub>62</sub>O<sub>14</sub>

Synonyms:C₆₉H₆₂O₁₄

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Chemical Property of C₆₉H₆₂O₁₄

Chemical Property:

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Technology Process of C₆₉H₆₂O₁₄

There total 13 articles about C₆₉H₆₂O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1599469-72-3
C₃₅H₃₀O₈

: 184698-69-9,159420-94-7
benzyl 2,3,4-tri-O-benzyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 1599469-73-4
C₆₉H₆₂O₁₄

: C₆₉H₆₂O₁₄

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃; Overall yield = 20 %; Overall yield = 60 mg; Inert atmosphere; Molecular sieve;

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 1599469-73-4
C₆₉H₆₂O₁₄

: C₆₉H₆₂O₁₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3.1: barium(II) hydroxide / methanol / 40 °C

4.1: sodium hydroxide; dihydrogen peroxide / methanol; water / 0 - 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 0.17 h / 20 °C

7.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -40 - 20 °C / Inert atmosphere; Molecular sieve

With hydrogenchloride; dmap; trimethylsilyl trifluoromethanesulfonate; dihydrogen peroxide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; barium(II) hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 100-44-7
benzyl chloride

: 1599469-73-4
C₆₉H₆₂O₁₄

: C₆₉H₆₂O₁₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3.1: barium(II) hydroxide / methanol / 40 °C

4.1: sodium hydroxide; dihydrogen peroxide / methanol; water / 0 - 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 0.17 h / 20 °C

7.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -40 - 20 °C / Inert atmosphere; Molecular sieve

With hydrogenchloride; dmap; trimethylsilyl trifluoromethanesulfonate; dihydrogen peroxide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; barium(II) hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;