ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate

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Chemical Name:ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate
CAS No.:1420536-74-8
Molecular Formula:C₂HF₃O₂*C₁₆H₂₁N₅O₂
Molecular Weight:429.399
Hs Code.:

Synonyms:ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate

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Chemical Property of ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate

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Technology Process of ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate

There total 2 articles about ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1420536-47-5
ethyl 2-((1-phenethyl-1H-tetrazol-5-yl)(tritylamino)methyl)cyclopropanecarboxylate

: 76-05-1
trifluoroacetic acid

: 1420536-74-8
ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 0.0166667h;
DOI:10.1021/ol303348m

Reference yield:

: 13949-93-4,13950-12-4,77183-91-6,77183-92-7,109716-50-9,109716-61-2,20417-61-2
ethyl-2-formyl-1-cyclopropane carboxylate

: 59795-89-0
phenethyl isocyanide

: 1420536-74-8
ethyl 2-(amino(1-phenethyl-1H-tetrazol-5-yl)methyl)cyclopropanecarboxylate 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 0.25 h / 100 °C / Microwave irradiation

1.2: 0.25 h / 100 °C / Microwave irradiation

2.1: dichloromethane / 0.02 h / 20 °C

In ethanol; dichloromethane; 1.1: |Ugi Condensation / 1.2: |Ugi Condensation;
DOI:10.1021/ol303348m