1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde

Base Information

Chemical Name:1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde
CAS No.:33040-02-7
Molecular Formula:C₁₄H₁₇FeNO
Molecular Weight:271.142
Hs Code.:

Synonyms:1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde

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Chemical Property of 1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde

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Technology Process of 1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde

There total 1 articles about 1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 109-72-8,29786-93-4
n-butyllithium

: 124944-44-1
1'-(tri-n-butylstannyl)-1-{(dimethylamino)methyl}ferrocene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 33040-02-7
1'-N,N-dimethylaminomethylferrocene-1-carbaldehyde

: 1461-25-2
tetra-n-butyltin(IV)

Guidance literature:: With water; In tetrahydrofuran; hexane; under N2 atm.; Teflon valved NMR tube was loaded with Fe complex; soln. of n-BuLi in hexane was added; THF added; NMR tube was shaken for several min; volatiles removed (vac.); solid dissolved in C6D6; DMF condensed into NMR tube; mixt. was shaken; H2O added; monitored by NMR spectroscopy;
DOI:10.1016/j.jorganchem.2005.10.034