Technology Process of C60H75NO18
There total 5 articles about C60H75NO18 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; dmap; pivaloyl chloride;
In
tetrahydrofuran;
at 35 ℃;
for 0.5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: camphor-10-sulfonic acid / acetonitrile / 0.58 h / 20 °C
2: trifluoroacetic acid / toluene / 14 °C
3: phenyllithium / tetrahydrofuran; dibutyl ether / 0.17 h / -60 °C / Inert atmosphere; Cooling with acetone-dry ice
4: dmap; 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 0.5 h / 35 °C / Inert atmosphere
With
4-methyl-morpholine; dmap; camphor-10-sulfonic acid; pivaloyl chloride; phenyllithium; trifluoroacetic acid;
In
tetrahydrofuran; dibutyl ether; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / toluene / 14 °C
2: phenyllithium / tetrahydrofuran; dibutyl ether / 0.17 h / -60 °C / Inert atmosphere; Cooling with acetone-dry ice
3: dmap; 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 0.5 h / 35 °C / Inert atmosphere
With
4-methyl-morpholine; dmap; pivaloyl chloride; phenyllithium; trifluoroacetic acid;
In
tetrahydrofuran; dibutyl ether; toluene;