Technology Process of C32H34
There total 4 articles about C32H34 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluorormethanesulfonic acid;
In
toluene;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1002/ejoc.201001484
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; sulfuric acid; copper; ammonium chloride; copper(l) chloride / 3 h
1.2: 168 h / 20 °C / Inert atmosphere
2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane; chloroform / 36 h / -78 - 20 °C / Molecular sieve; Inert atmosphere
3.1: tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
4.1: trifluorormethanesulfonic acid / toluene / 6 h / 20 °C / Inert atmosphere
With
hydrogenchloride; tetrapropylammonium perruthennate; trifluorormethanesulfonic acid; sulfuric acid; copper; ammonium chloride; 4-methylmorpholine N-oxide; copper(l) chloride;
In
tetrahydrofuran; dichloromethane; chloroform; toluene;
3.1: Grignard reaction;
DOI:10.1002/ejoc.201001484
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane; chloroform / 36 h / -78 - 20 °C / Molecular sieve; Inert atmosphere
2: tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
3: trifluorormethanesulfonic acid / toluene / 6 h / 20 °C / Inert atmosphere
With
tetrapropylammonium perruthennate; trifluorormethanesulfonic acid; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; chloroform; toluene;
2: Grignard reaction;
DOI:10.1002/ejoc.201001484
