1-benzyloxygenipin

Base Information

• Chemical Name: 1-benzyloxygenipin
• CAS No.: 206755-40-0
• Molecular Formula: C₁₈H₂₀O₅
• Molecular Weight: 316.354
• Mol file: 206755-40-0.mol

Synonyms:1-benzyloxygenipin

Chemical Property of 1-benzyloxygenipin

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-benzyloxygenipin

There total 3 articles about 1-benzyloxygenipin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

genipin (70094-79-0,73610-59-0,6902-77-8) + benzyl alcohol (100-51-6,185532-71-2) → 1-benzyloxygenipin (206755-40-0)

Guidance literature:

With hydrogenchloride; In water; for 5h; Reflux;

Reference yield: 56.0%

→ 1-benzyloxygenipin (206755-40-0)

Guidance literature:

With hydrogenchloride; In water; for 7h; Reflux;

Reference yield: 39.0%

(+)-genipin (224055-63-4) → methyl (1R,4AS,7AS)-1-benzyloxy-7-formyl-1,4a,5,7a-tetrahydrocyclopenta[c]pyran-4-carboxylate + 1-benzyloxygenipin (206755-40-0)

Guidance literature:

With benzyl alcohol; trifluoroboron diethylether; In tetrahydrofuran; ethyl acetate;

upstream raw materials:

(+)-genipin

genipin

benzyl alcohol

Refernces

• 1、 -. "Novel genipin derivatives and preparation method and application thereof". Paragraph 0263-0265. . Retrieved 2021/06/23.
• 2、 -. "Genipin derivative having anti hepatitis B virus activity". . . Retrieved 2008/06/13.