(2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

Base Information

Chemical Name:(2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine
CAS No.:140225-92-9
Molecular Formula:C₂₈H₂₅ClN₂O₅
Molecular Weight:504.97
Hs Code.:

Synonyms:(2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

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Chemical Property of (2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

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Technology Process of (2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

There total 3 articles about (2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1149724-09-3
1-(1H-benzo[d][1,2,3]triazol-1-yl)-2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]ethan-1-one

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 140225-92-9,76823-26-2
(2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

Guidance literature:: With triethylamine; In water; acetonitrile; at 20 ℃; for 16h;
DOI:10.1039/c4ob01681e

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 104425-42-5
[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetic acid 2,5-dioxopyrrolidin-1-yl ester

: 140225-92-9,76823-26-2
(2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

Guidance literature:: With borate buffer; In 1,4-dioxane; for 2h; Yield given;
DOI:10.1021/jm00085a012

Reference yield:

: 53-86-1
[1-(4-chlorobenzoyl)-5-methoxy-2-methylindol-3-yl]acetic acid

: 140225-92-9,76823-26-2
(2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DCC / 1.) 1,4-dioxane, 15 min, 2.) 1,4-dioxane, 24 h

2: borate buffer (pH 8.5) / dioxane / 2 h

With borate buffer; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jm00085a012